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LABORATORY SYSTEM - YES LABKOTE |
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VAPOR
DEPOSITION SYSTEMS |
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Whether you need a
moisture resistant barrier or a reactive surface for your application,
the YES-LabKote is especially suited for achieving uniform results. This
compact, tabletop unit is ideal for Research & Development laboratories
and pilot line production.
There is a growing need for precise control over nanoscale surface
areas. The YES-LabKote is designed to accommodate a variety of
functionally diverse silanes for a variety of processes on a multitude
of surfaces. The system can accommodate the use of silanes ranging from
non-reactive adhesion promoting coatings such as HMDS to alkyl silanes
such as OTS to more reactive chemistries such as amines, acrylates or
epoxies. For anti-stiction applications, fluorinated silanes can be
used.
The efficient use of chemical allows coatings using as little as 100µL
of chemical. At the same time, the 8"x8"x6" chamber can accommodate
several hundred glass slides or oddly shaped substrates in a
pre-production mode. For higher volume production, a developed process
can be directly transferred to the YES-1224P system.
The linked recipes allow the user to easily go from hydration to
deposition without breaking vacuum. The linking also allows for
sequential deposition, reacting one silane with another or passivating
the chemistry at the end of the deposition with a reducing plasma to
ensure a known surface. |
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TYPICAL APPLICATIONS |
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YES
LabKote chemical vapor deposition (CVD) system |
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MEMS packaging |
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Semiconductor
fabrication |
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Microarrays |
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DNA microarrays |
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Protein
microarrays |
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BioMEMS |
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Achieving
biocompatibility |
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BENEFITS |
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Efficient chemical usage |
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Repeatability – Substrate to
substrate, run to run |
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Superior uniform coatings |
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Minimal waste |
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Vacuum dehydration |
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Process flexibility |
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Cost savings/Fast ROI |
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Reliability |
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Batch process |
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SOFTWARE OPTIONS |
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INFORMATION
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to
Process
Management Software |
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to YES
Info Page |
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INFORMATION
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SPECIFICATION SHEETS |
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Model
YES-LabKote - Technical Note  |
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SILANE VAPOR
DEPOSITION PROCESS |
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Dehydration followed
by silane vapor deposition coating provides a superior silane/substrate
bond that is stable after exposure to atmospheric moisture, extending
the time available between process steps. The silane vapor deposition
process begins with vacuum chamber cycle purges to prepare the
substrates. The chamber is evacuated to low pressure and refilled with
pure nitrogen several times to completely remove water vapor and oxygen.
Nitrogen is preheated which helps heat slides and chips. Once cycle
purges are finished the YES-LabKote system pumps the chemical directly
from the source bottle to the heated vaporization chamber – without
exposing the chemical to moisture or oxygen. |
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SUMMARY |
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Successful surface
modification requires stringent control of the interaction between the
silane and substrates they contact. Using the YES-LabKote system you
will achieve your specific results – with less chemical usage. |
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MANUAL SYSTEM - YES 1224P (WITH PLASMA) |
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VAPOR
DEPOSITION SYSTEMS |
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YES vapor deposition
systems provide total environmental control over the deposition process
and accommodate a variety of functionally diverse silanes, for a variety
of processes, on a variety of surfaces. |
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GIVES PROCESS CONTROL OVER |
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YES
1224P chemical vapor deposition (CVD) system |
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Amount of liquid |
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Speed of liquid injection |
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Vaporization chamber temperature |
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Vapor line temperature |
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Process vacuum chamber temperature |
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Process starting pressure |
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Exposure time |
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Surface preparation |
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APPLICATIONS |
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Surface modification to prevent or
promote adhesion |
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Photoresist adhesion for
semiconductor wafers |
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Silane/substrate adhesion for
microarrays (DNA, gene, protein, antibody, tissue)
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MEMS coating to reduce stiction
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BioMEMS and biosensor coating to
reduce "drift" in device performance |
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Promote biocompatibility between
natural and synthetic materials |
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Copper capping
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Anti-corrosive coating
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SOFTWARE OPTIONS |
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INFORMATION
|
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to
Process
Management Software |
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to YES
Info Page |
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SOFTWARE OPTIONS |
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SPECIFICATION SHEETS |
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Model
YES-1224P - Technical Note 
Surface tension
modification for
Biotech Industry
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VAPOR
DEPOSITION PROCESS |
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Dehydration followed
by silane vapor deposition coating provides a superior silane/substrate
bond that is stable after exposure to atmospheric moisture, extending
the time available between process steps. Chemical usage for a vapor
deposition process is typically less than 1% of the amount needed for
wet application processes, significantly reducing waste and chemical
costs.
The vapor deposition process begins with vacuum chamber cycle purges to
dehydrate the product. The chamber is evacuated to low pressure and
refilled with pure nitrogen several times to completely remove water
vapor. Nitrogen is preheated, which helps heat the product.
Once cycle purges are finished, the YES-1224P system pumps the chemical
directly from the source bottle to the heated vaporization chamber
without exposing the chemical to moisture.
YES-1224P accommodates two chemical source bottles (option for 3) as
well as wide variations of vapor pressures among different silanes.
Processes are easily programmed using a touch screen operator interface. |
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PLASMA PROCESS |
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Plasma cleaning prior
to silane deposition improves repeatability. Plasma cleaning the process
chamber before each run ensures all runs start from the same point.
Additionally, plasma prepares the substrate for deposition. interface. |
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SILANE VAPOR
DEPOSITION SYSTEMS BENEFITS |
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Chemical
deposition uniformity |
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Contact angle
control within +/- 3 degrees |
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Moisture
resistant surface modification |
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More time
available between process steps |
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Promotes
Silane/substrate bonds |
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Angstrom-level
thickness control |
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Hexamethyldisilizane (HMDS)/wafer bonds will last for weeks with
no change to surface adhesion |
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Increased MEMS
and bioMEMS reliability |
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Reduced
chemical usage over wet chemical modification |
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MEMS APPLICATIONS |
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WAFER DEHYDRATION |
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The moisture on the surface of wafers
will cause unintended reactions with various deposition steps. These
reactions result in unstable surface which degrade over time. Vacuum
dehydration provides a clean stable starting surface resulting in
superior films. |
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SURFACE TENSION MODIFICATION |
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As devices are made smaller and smaller,
static friction (stiction) becomes more and more significant. By
modifying the surface tension with a class of fluorinated silanes, the
operating life of moving parts in MEMS devices can be significantly
lengthened. Conversely, if surfaces need to be bonded together, other
silanes can be coated which enhance bonding strengths between unlike
materials. |
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SILYLATION |
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YES-1224P can also be
used as a silylation oven. This process enables the use of short
wavelength radiation with its attendant shallow depth of field to
define high-resolution photoresist topographies.
The process requires exposure of the photoresist layer using a standard
process with a reverse mask of the circuit. The wavelength is used to
irradiate the top level of exposed photoresist. Now, the substrate is
moved to the silylation oven to be exposed to HMDS vapor.
Indene-carboxylic acid generated where the photoresist was exposed then
combines with HMDS vapor, impregnating the shallow surface layer with
pure silicon.
In the subsequent oxygen plasma process, this silicon layer forms an
effective mask and is converted to silicon dioxide. The plasma removed
only the unexposed photoresist, leaving a high resolution profile of the
defined circuit. |
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